High Pressure Milling Vial
EVICO Magnetics High Pressure Milling Vial is a system for reactive ball milling under high hydrogen atmosphere with in-situ monitoring of temperature and hydrogen pressure, ext...
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A method for the synthesis of hydrogen storage materials and monitoring of hydrogenation reactions by reactive ball milling under high hydrogen atmosphere uses an especially designed vial.
The system allows in-situ monitoring of temperature and hydrogen pressure by incorporating a gas-temperature measurement system and a radio emitter into the vial lid.
An external receiver transmits the data to a data acquisition computer.
The page lists applications including insight into physical and chemical processes during high-energy ball milling, quick check of catalytic efficiency, and accelerated hydride formation and nanocrystallinity.
Options include a two channel system for simultaneous use of two milling vials.
| Pressure monitoring | Continuous in-situ monitoring of pressure and temperature during ball milling |
|---|---|
| Maximum hydrogen pressure | 150 bar bar |
| Available pressure ranges | 1, 2, 5, 10, 20, 50 and 100 bar smaller pressure ranges with higher resolution available bar |
| Operation time | up to 40 h h |
| Data acquisition resolution | 40 points/s points/s |
| Interface | USB interface |
| Milling vial volume | 220 ml ml |
| Vial material | hardened steel, Swagelok ball valve |
| Software | Powerful dedicated software |
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